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ADFlex Solutions Ltd

Report on solder recycled by solder recovery system

INTRODUCTION

Circuits were soldered using 100% recovered solder in a solder fountain system, representative of the wave solder system and using the same flux. Component analysed was a 30 pin through hole connector.

REPORT

Visual examination at up to 40x mag. showed that all the solder was smooth, shiny, bright and showed good wetting. No solder splashes or residues were observed.

Examination of microsectioned soldered areas showed there to be good wetting. Compositional analysis of microsectioned solder areas by ZAF analysis gave the following results:

  Element percentage
Lead
46.4
Tin
53.6

CONCLUSION

Overall the results obtained indicate the visual solder quality to be acceptable.

INTRODUCTION (2nd Part)

A sample of recovered solder was submitted for compositional analysis by XRF.

Date submitted: 01/07/97

REPORT

The sample was analysed by XRF against appropriate analytical standards and the results obtained were:

Cu 0.03x
Sn 62.6x
Au <0.01x

CONCLUSION

The recovered solder bar shows tin concentration to be consistent with normal production solder.

The initial work above details SEM/ZAF correction analysis of solder joints which show compositional analysis of microsectioned solder areas by ZAF analysis.

Discrepancies between XRF (bulk analysis) and SEM/ZAF (spot analysis) are believed accounted for from the analysis of sectioned samples which are subject to local concentration gradients across grain boundaries after tin migration during solder reflow.

Derek Morgan
ADFlex Solutions Ltd
Process Engineering
Dept. 194, Area 26/22
PO BOX 6, Havant, Hampshire
United Kingdom

 

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